Lab handouts

 

Date

Lab

Assignment Due in your lab section:

Week 1: Jan 12

Check-In

1.Biginelli Reaction

(Multicomponent Coupling)

 

 

Week 2: Jan 19 MLK Jr. Day  

Week 3: Jan 26

2. Phenylalanine substitution

 Lab notebook:  Biginelli (Multicomponent Coupling) reaction

Week 4: Feb 2

2. Continue Phe substitution

 

Week 5: Feb 9

3. Suzuki Cross coupling Formal Report: Phe Substitution

Week 6: Feb 16

4. Stereochemistry of Benzil Reduction  

Week 7: Feb 23

4. Continue Stereochemistry of Benzil Reduction Optional: Suzuki report/poster

Week 8: Mar 2

5. Elimination of Tosylates

Hickman Still

Optional: Benzil reduction report/poster

Week 9: Mar 9

5. Continue Elimination of Tosylates

 

Week 10: Mar 23

6.. Kinetic vs Thermodynamic control

 

Optional: Elimination of tosylates report/poster

Week 11: Mar 30

6.. continue Kinetic vs Thermodynamic control

 

Week 12: Apr 6

7.  Solvent KIE of hydrolysis Optional: Kinetic vs. Thermodynamic report/poster

Week 13: Apr 13

8. LFER competition

 

Week 14: Apr 20

8. continue LFER competition

 

Week 15: Apr 27

Checkout Optional: LFER report/poster