Date |
Topic
|
Notes |
Supplementals |
| Week 1 | Prelabs are due every Wed at midnight. LABS in WEEK 1 MEET to do drawer check-in & safety training |
Turnitin Instructions Updated with Jing and Lauren's section correct new lab times | |
| 9/1 | Introduction (syllabus, lab reports & lab safety) | Organic Lab Reports Guidelines Free Radical Halogenation Lab Handout due week 3 in lab |
|
| 9/3 | 4.4: Simple & Fractional Distillation | ||
| Week 2 | Labs perform simple & fractional distillation | ||
| 9/8 | Infrared Spectroscopy | ||
| 9/10 | 6.2 & 6.3: TLC & Column Chromatography | ||
| Week 3 | Labs perform TLC & CC | Distillation summary & FRH lab report due in lab | |
| 9/15 | Finish Infrared Spectroscopy notes |
IR Worksheet - due 9/29 |
|
| 9/17 | 5.3A: Acid & Base Extractions Read 2.17 on filtration, too (not on syllabus) |
You will get a worksheet from your AI in lab next week to fill out and hand in during week 5. |
|
| Week 4 | Labs perform extraction lab | TLC/CC summary due in lab | |
| 9/22 | Introduction to NMR Spectroscopy & Carbon-13 Spectroscopy (chapter 8.3 NMR in G&M) |
Carbon Worksheet - due 10/15 |
|
| 9/24 | 17.4: Reduction of 9-Fluorenone |
||
| Week 5 | Labs perform reduction of fluorenone & finish up extraction lab identifications | Nothing due in lab, but WS1 and quiz 1 in class | |
| 9/29 | Carbon-13 Spectroscopy IR worksheet due in class |
||
| 10/1 | 16.2A: Oxidation of Alcohols Quiz 1 on IR Spectroscopy |
||
| Quiz 1 distibution, average 21/30 | |||
| Week 6 | Labs perform oxidation of alcohols | Reduction WS due inlab (If you are done with the Extraction WS, I would advise you handing it in, otherwise it's due in Week 7) | |
| 10/6 | Carbon-13 Spectroscopy | ||
| 10/8 | Base-promoted Elimination of RX Quiz 2 on Techniques Distillation, TLC, CC, Extractions and Recrystallization |
Prelab 6, KEY | |
| Quiz 2 distibution, average 22.5/30 | |||
| Week 7 | Labs perform Elimination of RX | Extraction WS due if not already handed in, and Oxidation of ROH full lab report due in lab | |
| 10/13 | Finish Carbon-13 Spectroscopy and start Hydrogen-1 Spectroscopy |
||
| 10/15 | Hydrogen-1 Spectroscopy 13C worksheet due in class |
Complex splitting patterns in proton NMR | |
| Week 8 | No labs run during exam week | No labs running and no labs due | |
| 10/20 | Review for Exam Bring your questions with you. |
1H NMR Worskheet - due 11/19 |
|
| 10/20 | Exam 1: 7:15 - 9:15 pm Topics include: IR spectroscopy, carbon-13, and the first five labs: distillation, TLC/CC, extraction/recrystallization, reduction and oxidation labs. |
NO PROTON NMR WILL BE ON THE EXAM.
|
|
| 10/22 | 10.7: Hydration of Norbornene | ||
|
Average (115/150) |
|||
| Week 9 | Labs perform Hydration of Norbornene | Elimination of RX lab report due in lab | |
| 10/27 | Hydrogen-1 Spectroscopy | ||
| 10/28 | Last day to drop with an automatic "W" | ||
| 10/29 | 12.3B: Diels-Alder Reaction | ||
Don't forget about the |
|||
| Week 10 | Labs perform Diels-Alder reaction | Norbornene summary due in lab | |
| 11/3 | Hydrogen-1 Spectroscopy | ||
| 11/5 | 20.2: Fisher Esterification Quiz 3 on proton NMR |
||
| Quiz 3 Distribution, average 25/30 | |||
| Week 11 | Labs perform esterification reaction | Diels-Alder summary due in lab | |
| 11/10 | Mass Spectrometry | Mass Spec Worksheet - due 12/4/09 by 4 pm in C021 | |
| 11/12 | 19.4A: Preparation of Triphenylmethanol | Prelab 10 | |
| Week 12 | Labs perform Grignard lab | Fisher Esrerification lab report due in lab | |
| 11/17 | Mass Spectrometry | ||
| 11/19 | 15.4: Nitration of Bromobenzene 1H worksheet due in class (or earlier) |
Prelab 11 (yes, it really is the last one) | |
| Week 13 | No labs running and nothing due this week | ||
| 11/24 | Lecture Cancelled | ||
| 11/26 | Thanksgiving Break | ||
| Week 14 | Labs perform electrophilic arom. substitution |
Grignard lab report due in lab | |
| 12/1 | Mass Spectrometry | More online integrated problems | |
| 12/3 | Mass Spectrometry Quiz 4 on experiments : elimination, hydration, Diels-Alder, Grignard |
||
| 12/4 | MS worksheet due by 4 pm to UGO or in lecture on 12/10 | ||
| Week 15 | Lab check-out - YOU MUST SHOW UP TO LAB TO CHECK OUT! | EAS WS due in lab before leaving this week | |
| 12/8 | Mass Spectrometry | ||
| 12/10 | Practice Spectroscopy Problems MS worksheet due by 4 pm to UGO or in lecture on 12/10 |
||
| 12/17 | Exam 2, 2:45-4:45 p.m. |
Department of Chemistry | College of Arts and Sciences | Chemistry Library | OneStart | Personnel | CALM | Comments
800 E. Kirkwood Ave., Bloomington, IN 47405-7102 | Ph: (812) 855-9043 | Fx: (812) 855-8300
Copyright © 2009 | The Trustees of Indiana University | Copyright Complaints
Last Modified: Friday, November 20, 2009 XHTML / CSS
Designed and developed by Kevin Joseph Ruble in September 2008.